含筋率和弹着点对钢筋混凝土抗侵彻性能的影响

阐述了侵彻钢筋混凝土几种常用的建模方法,选用AUTODYN中的Lagrange算法,对已有的动能弹侵彻钢筋混凝土问题进行了计算,计算结果与试验数据符合较好。使用此方法,分析了含筋率和配筋方式对钢筋混凝土靶抗侵彻性能的影响,以及弹着点对动能弹侵彻性能的影响。研究表明,钢筋越粗或者钢筋编织越密,即含筋率越高,钢筋混凝土靶板的抗侵彻能力越强,尤其对于动能弹直径大于靶板中钢筋间距的情况,效果明显;另外,弹着点对动能弹侵彻能力有较大影响。 更多还原     

Evaluation of important fatty acid ratios in poultry feed lipids by ATR FTIR spectroscopy

A rapid, simple and reproducible single bounce attenuated total reflectance (SB-ATR) Fourier transform infrared (FTIR) spectroscopic method was developed for determination of the n − 6, n − 3 and ratio of n − 6:n − 3 polyunsaturated fatty acids (PUFAs) in poultry feed lipids using partial least squares (PLS) regression. Data for n − 6, n − 3 and ratio of n − 6:n − 3 was acquired by gas chromatography (GC) and used as a standard values for FTIR calibration. The best regression results were achieved using first derivatives of the 1475–650 cm⁻¹ spectral region for n − 6, n − 3 and ratio of n − 6:n − 3 with high regression coefficients (R²) of 0.999, 0.994 and 0.998, respectively and low RMSEP values of 1, 0.06 and 0.83, respectively. The results of the present study revealed that FTIR could be used for rapid and accurate determination of n − 6, n − 3 and ratio of n − 6:n − 3 PUFAs present in poultry feed lipids.     

Fe3O4磁液的悬浮率测定及稳定性研究

The paper first reported the preparation of ultrafine Fe₃O₄ powder about 8～10nm by improved chemical pre-cipitation method， then turned it into magnetic fluid. The phase analysis， morphology， ultrafine powder size and magnetic property were measured by XRD， TEM and vibrating sample magnetometer(VSM)，respectively. In ad-dition， a new method ， by analyzed the suspending percentage of Fe₃O₄ powder， was introduced to study the effects of concentration， pH value， centrifugal rate and time on the stability of the magnetic fluid.     

Characterization of Hydrocarbon Soluble Metal Oxides. Precursors to Supported Catalysts

Abstract

The metal oxide carboxylate complexes described in the previous chapter have been characterized by infrared spectroscopy, x-ray diffraction, electron microscopy, and analytical ultracentrifugation. The molecular weights and solution particle diameters have been determined for a number of the hydrocarbon soluble particles by analytical ultracentrifugation methods, and the use of a spherical model consistent with the particulate shape observed by electron microscopy. The size of the soluble complexes has been studied as a function of: metal, metal/acid ratio, acid composition, and solvent. The molecular weights for the ultimate particles are reasonably independent of the metal employed in the synthesis and are relatively constant for materials with similar metal/acid equivalents ratios. The single particle molecular weights for the complexes studied ranged from approximately 5×10⁴ to 1.5×10⁶g mole^?1. The solution size distribution was polydisperse in all cases, with aggregates of the ultimate particles prevalent. Weight average molecular weights in excess of 10⁹g mole^?1 have been observed. The aggregation is dependent on the surface acid composition and on the solvent in which the soluble complex is dispersed. Solubility and stability of these materials have been examined in a number of solvents. The metal oxide particles are initially soluble in octane, isooctane, cyclohexane, mineral spirits, carbon tetrachloride, benzene, and tetrahydrofuran. However, most of the complexes eventually precipitate from dilute solutions in carbon tetrachloride, benzene, and tetrahydrofuran. The stability of the particles is decreased in the presence of oxygen, or when carboxylic acids, alcohols, or ketones are present even in small amounts, and is decreased even further at temperatures above 100°C. Heterogeneous catalysts have been prepared by deposition of several of the soluble metal oxides onto supports such as alumina, silica, or kieselguhr followed by oxidation to yield supported metal oxides or reduction to yield supported metal. The application of few supported metals and metal oxides in hydrogenations of olefins, benzene, and naphthalene is described.     

含氮杂环的芳甲酰基硫脲的合成及其生物活性

合成了7个新的含安替比林基的芳甲酰基硫脲类化合物（5a-5g）,其结构经^1H NMR,IR和元素分析确证。对5进行的室内生物活性测试结果表明,部分5对某些真菌具有较高的抑菌率,其中5c和5f对黄瓜灰霉的抑菌率分别达到96．23％和94．34％。     

露天煤矿的台阶高度对抛掷率的影响

以黑岱沟露天煤矿为例,在理论分析和现场实验的基础上,探讨台阶高度对抛掷爆破效果的影响。 现场实验结果表明:爆堆最远抛距和抛掷率随台阶高度的增加而增大,爆堆形态也变得更平滑;随台阶高度 的进一步增加,抛掷率增大的幅度逐渐减小。当炸药单耗q=0.70kg/m3,台阶高度H 37m 时,随台阶高 度的增大,抛掷率的提高不明显,甚至是停留在47%左右,此时单靠提高台阶高度来获取较高抛掷率的方法 将受采场条件和钻采机械设备的限制。     

红外光学系统的污染镜面杂散辐射分析

以卡塞格伦结构为例,利用ASAP光学分析软件,建立了红外光学系统的三维仿真模型,在光学元件表面存在均匀分布和非均匀分布的微粒污染情况下,对红外光学系统的杂散辐射特性进行了仿真和比较分析,对影响系统杂散辐射特性的主要因素进行了讨论,并对系统中机械元件的杂散辐射路径进行了分析。在此基础上,采用有效发射率对系统的杂散辐射性能进行了评价,讨论了镜面污染程度对红外光学系统杂散辐射性能的影响。     

作物植被覆盖度的高光谱遥感估算模型

通过大田试验,使用ASD光谱仪测量了油菜、玉米、水稻三种作物不同覆盖度水平下的冠层光谱,同时拍照获取植被图片并用计算机求算了植被覆盖度。利用三种作物光谱求算“红边”变量,并对波段两两组合求算归一化植被指数(NDVI),建立这些光谱变量与覆盖度之间的估算模型,得到适用于三种作物的最优估算模型和最佳的NDVI波段组合。另外,利用响应函数模拟了TM归一化植被指数,同植被覆盖度进行了相关分析,回归方程的R2达到0.80,并通过了预留数据的检验,为TM数据植被覆盖度估算进行了探索性的研究。     

罗丹明6G缔合微粒光度法检测羟自由基及其在离体筛选抗氧化剂中的应用

在HCl-NaAc缓冲溶液中,Fenton反应产生的羟自由基被过量的KI捕获;生成的I-₃分别与罗丹明B(λ_max=554 nm)、罗丹明6G(λ_max=526 nm)、罗丹明S(λ_max=526 nm)和丁基罗丹明B(λ_max=556 nm)形成缔合微粒,导致其吸收峰降低。羟自由基浓度(以H₂O₂浓度计)分别在0.136～0.68 μg·mL-1,0.064～0.680 μg·mL-1,0.064～0.680 μg·mL-1和0.064～0.680 μg·mL-1范围内与罗丹明B、罗丹明6G、罗丹明S和丁基罗丹明B体系的吸光度降低值成正比。据此建立了一种测定抗氧化剂对羟自由基的清除率的新方法。测试了抗坏血酸等4种抗氧化剂以及6种茶叶提取液的抗氧化活性,所得到的结果较为满意。